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Tech Focus: "How Long Is a Mile?"

The Importance of Calibration
by Air Hygiene Lab Manager Mars Sharief


The development of measurements and standardization of measurements took mankind several thousand years. An object can be described by its weight, length, area it occupies, density, etc. There are several ways to measure the weight of the object. It can be measured in terms of kilograms, pounds, tons, ounces, etc. In the United States, the National Institute of Standards and Technology standardizes the units of measurement.

The quality of the measurement depends upon the calibration and units of the measuring device. For example, an imperial gallon used to measure volume in Great Britain is not the same as the U.S. gallon. In fact, the U.S. gallon is smaller.

Air Hygiene uses separate analyzers to characterize the emission gases. Some of these gases include carbon dioxide (CO2), carbon monoxide (CO), oxygen (O2), oxides of nitrogen (NOx), total hydrocarbons (THC), sulfur dioxide (SO2), and hydrogen sulfide (H2S). The various analyzers (O2, CO2, NOx, CO, THC, SO2) used at to quantify the emissions have a tendency to drift as a function of time, pressure, and temperature. Therefore, a calibration is performed at the beginning of each day.

Calibrations are carried out on each measurement device according to the schedule outlined by the Environmental Protection Agency. The gases used to perform calibration have previously been tested and certified for specific concentration as marked on the bottle by the vendor. The vendor also provides a preparation date and an expiration date along with the concentrations and the contents of the gas bottle. A gas that has expired is not valid for calibration; therefore, quality control is necessary.

At Air Hygiene, the emission testing analyzers are calibrated at the beginning of each day, before testing. First, the analyzer is set to zero concentration by sending Nitrogen gas or zero concentration of the gas of interest. Second, the analyzer is once again adjusted with the span concentration of gas of interest. Finally, the analyzer is checked with one or two mid concentrations of gas. A linearity test is performed to check whether the calibration was successful. If the calibration does not pass the linearity test, the process is repeated.

An erroneous calibration can lead to an erroneous test. Therefore, quality control is necessary. At Air Hygiene, quality control checks are also conducted in the field for each test program. The company conducts air emission testing services per the requirements of the Environmental Protection Agency and other relevant organizations such as State Environmental Departments, the American Society for Testing and Materials (ASTM) and the Gas Processors Association (GPA). The company has a Standard Operating Procedures Manual and a QA/QC program to establish accuracy of the testing results and to insure confidence to the customer.



 
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